E – 02 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, and Cobalt Alloys, cobalt alloys. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion.
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Note 22—The upper limit of the scope has been set at 0. Solid samples may be analyzed in either automatic or manual mode, but drillings or chips should be analyzed in the manual mode.
Test the furnace and the analyzer to ensure the absence of leaks. However, recognizing that commercial nitrogen determinators are capable of handling higher concentrations, this test method provides a calibration procedure up to 0.
The value should agree with r1019 assigned value for Calibrant C within a range of 6 s, the standard deviation of a single determination of Calibrant C using this method.
If samples are to be analyzed in the manual mode, blank determination and calibration should be performed r1019 the manual mode. It is expected that work will be performed in a properly equipped laboratory. Standards Subscriptions from ANSI provides a money-saving, multi-user solution for accessing standards. The use of small and irregular shaped samples requires a diligent effort to ensure that all surface contamination has been removed. Thus, the absorption of IR energy can be attributed to only CO2 and its concentration is measured as changes in energy at the detector.
The SO2 is measured with a solid state energy detector, and lters are used to pass the appropriate IR wavelength to the detector.
Use a fresh crucible each time Note This standard is also available to be included in Standards Subscriptions. As the voice of the U. Please first verify your email before subscribing to alerts.
The IR absorption properties of the SO2 gas in the chamber cause a qstm of energy during combustion; a loss in signal, therefore, results that is proportional to the concentration of the gas in the closed loop. It is the responsibility of the user of this standard e10119 establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
The asym should be within e10119 allowable limits of the certied value.
This creates an IR energy imbalance reaching the diaphragm, thus distorting it. For other sizes, please contact us. Subscription pricing is determined by: Ni-base analyses are mainly performed as analyses of steel.
Blank values are equal to the total result from the crucible and Calibrant A minus the certied oxygen e10019 of Calibrant A. Use crucible tongs to handle the preburned crucibles. NOTE 9—This procedure is for analysis of steel samples and a new blank must be determined using 1. Blank values are equal to the total result of the accelerator and Calibrant A minus the certied value for the certied reference material.
Using a le, abrade the surface of the specimen to be used for analysis to remove oxides and other impurities, rinse in acetone, air dry, and weigh. Repeat a sufficient number of times to establish that a low average blank value 0.
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However, recognizing that commercial oxygen determinators are capable of handling higher concentrations, it may be that this test method can be used for oxygen concentrations outside of the scope.
Adjust the signal astj provide a reading within Preparation of Apparatus Comment 1 g sample 1 g sample. NOTE 22—The uncertainty of results obtained using this test method is dependent on the uncertainty of the values assigned to the calibration reference materials. The detector response data are processed and displayed directly as percent oxygen. Basic open hearth steel SRM 11h, 0. NOTE 11—The upper limit of the scope has been set at 0. Testing was performed in compliance with Practice E If you feel that your comments have not received a fair hearing you should make your views known to the ASTM Committee on Standards, at the address shown below.
Analyze at least three reference material specimens to determine calibration slope. All testing meets the requirements of Practice E Total sulfur, as SO2, is monitored and measured over a period of time. Blank values are equal to the total result of the accelerator and Calibrant A minus the certied value for the calibrant. As written, this test method is not applicable to cast iron samples.
In these cases, the removal of too much surface material may cause erroneous results. NOTE 23—If the unit does not have this function, the blank value must be subtracted from e119 total result prior to any calculation.
Crucibles must be composed of high purity graphite. Test Method B—The combustion is performed in a closed loop in which SO2 is detected astj an infrared cell. Standards Subscriptions from ANSI provides a money-saving, multi-user solution for accessing standards. Already Subscribed to this document. NOTE 27—The uncertainty of results obtained using this test method is dependent on the uncertainty of the values assigned to the calibration reference materials.
Treat each specimen as directed in Add to Alert PDF.
No other units of measurement are included in this standard. Electrolytic iron NBS0. The sulfur is then determined by infrared absorption.